Oleflex Process Robustness, Sn 10ID August 2011
Projects
Previous Studies
Notes
Experiments not run due to time constraints
Sn 2-fluor, Reduction Experiment
Sn EDGE, Reduction Experiment |
|||||||
# |
filename |
description |
Temp |
Gas |
EXAFS/XANES |
DONE |
PIC |
DeH-14 theta (lot#3032006026) |
|
||||||
Sn-only base As reference for Sn in PtSn Catalysts |
|
||||||
step 1 |
11Aug_Snx.00x-00x |
As Received at RT in He |
RT |
100% He |
9 EXAFS |
|
|
step 1 |
11Aug_Snx.00x-00x |
As Received at RT in He |
RT |
100% He |
9 EXAFS |
|
|
step 2 |
Reduce: Ramp to 550C at 5deg/min in 100% H2, dwell 30 min |
||||||
step 2 |
Start H2 wait 5 minutes then start ramp and data collection |
||||||
step 2 |
11Aug_Snx.00x-00x |
during reduction |
RT to 550 |
100% H2 |
EXAFS |
|
|
step 2 |
11Aug_Snx.00x-00x |
during reduction |
RT to 550 |
100% H2 |
EXAFS |
|
|
step 3 |
Cool to RT in H2 |
||||||
step 3 |
11Aug_Snx.0xx-0xx |
EXAFS after reduction |
RT |
100% H2 |
9 EXAFS |
|
|
step 3 |
11Aug_Snx.0xx-0xx |
EXAFS after reduction |
RT |
100% H2 |
9 EXAFS |
|
|