Pt/R9
Projects
Notes
# |
filename |
description |
Temp |
Gas |
EXAFS/XANES |
DONE |
PIC |
R-9-9 (Pt / R9) |
450mg in Quartz holder |
||||||
step 1 |
09aug_PtL3.008 |
As Rec, RT in He |
RT |
100%He |
PtL3 Exafs |
Done |
|
step 2 |
Ramp to 565C in H00% H2 @ 5C/min. 15 min Dwell |
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step 3 |
09aug_PtL3.009-023 |
PtL3 Xanes during TPR |
RT to 565C |
100% H2 |
PtL3-Xanes |
Done |
|
step 4 |
Cool to RT in H2 |
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step 5 |
09aug_PtL3.024-027 |
PtL3 After reduction. RT in H2 |
RT |
100% H2 |
PtL3 Exafs |
Done |
|
step 6 |
09aug_PtL2.004-005 |
PtL2 Xanes after reduction. RT in H2 |
RT |
100% H2 |
PtL2 XANES |
Done |
|
step 7 |
Ramp to 400C @ 5C/min in 100% He |
||||||
step 8 |
09aug_PtL2.006-022 |
PtL2 Xanes During H2 Desorption |
RT to 400C |
100% He |
PtL2 XANES |
Done |
|
# |
filename |
description |
Temp |
Gas |
EXAFS/XANES |
DONE |
PIC |
R-9-9 (Pt / R9) |
~450mg in Quartz holder |
||||||
step 1a |
09aug_PtL3.029 |
As Rec, RT in He |
RT |
100%He |
PtL3 Exafs |
done |
|
step 1b |
09aug_PtL2.023-025 |
As Rec, RT in He |
RT |
100%He |
PtL2 XANES |
done |
|
step 2 |
Ramp to 300C in H00% H2 @ 5C/min. 5 min Dwell |
||||||
step 3 |
09aug_PtL2.026-033 |
PtL2 Xanes during TPR |
RT to 300C |
100% H2 |
PtL2-XANES |
|
|
step 4 |
Cool to RT in H2 |
||||||
step 5 |
09aug_PtL3.030-033 |
PtL3 After reduction. RT in H2 |
RT |
100% H2 |
PtL3 Exafs |
done |
|
step 6 |
09aug_PtL2.034-035 |
PtL2 Xanes after reduction. RT in H2 |
RT |
100% H2 |
PtL2 XANES |
done |
|
step 7 |
Ramp to 400C @ 5C/min in 100% He |
||||||
step 8 |
09aug_PtL2.XXXX |
PtL2 Xanes During H2 Desorption |
RT to 400C |
100% He |
PtL2 XANES |
out of time |
|
